| Carbon Black is produced by partial
combustion of oils and pyrolysis in the reactor. Carbon
Black feed stock is suitably blended before charging into
the reactors. Predetermined quantities of process air
from a process air header system, fuel natural gas and
Carbon Black feedstock are introduced into the reactor,
which has been brought up to the desired temperature level.
At the initial stage, carbon nuclei or
precursors formed from the oil combine to form aggregates.
The reaction is stopped at suitable points by direct
quenching with water, at predetermined locations with
predetermined quantities. The entire operation of flow,
including the temperature measurements is controlled
by computer-supervised electronic instrumentation.
Effluents from the reactors are essentially
carbon-laden flue gases containing some combustibles.
These gases are at a temperature between 700oC and 900oC.
This heat is first utilised in preheating incoming process
air in an air preheater and then reused to heat incoming
Carbon Black feed stock in an oil preheater. This process
maximises heat recovery and process efficiency. The
effluents from the reactors pass into an inline boiler
and then into a common header called smoke header.
The smoke header leads the carbon-laden
flue into the main bag filter. Inlet of the flue is
controlled at about 280oC. The main bag filter is a
filter house consisting of multi-cylinders, where Carbon
Black is filtered. Clean gases containing combustibles
pass out of the filter to the Carbon Black pellet dryer.
Carbon black is recovered from the bag filters by reverse
flow of the flue gases into the cylinders, performed
in rotation one at a time. Carbon Black thus released
from the bags accumulates in the hopper and is dropped
into a pneumatic conveying line through air lock valves.
Two pneumatic conveying fans draw carbon black from
underneath the hopper.
Loose Carbon Black and the conveying gases
are drawn through two micro pulverisers and transferred
to the accumulator tank through a conveying cyclone
separator. The purpose of this cyclone is to separate
Carbon Black from the conveying gas. Loose Carbon Black
from the cyclone separator falls into the accumulator
tank and the conveying gas is drawn by a return fan
and returned to the smoke header at the bag filter inlet.
Carbon Black collected in the accumulator
tank is in a fluffy, powdery form, and being difficult
to handle as such, has to be pelletised. Pelletisation
is achieved in a proprietary machine called wet pelletiser
where the loose Carbon Black is mixed with a near equal
quantity of water and small quantities of pellet binders.
An indirectly fired rotary drum dryer is used to dry
the wet pellets. Drying is achieved by burning the part
of the waste gases from the main bag filter in a specially
designed combustor. Water vapour from the dryer is drawn
by an exhaust blower and the exhaust or purge gas exits
to the atmosphere.
The entire operation is completely automatic,
achieved by sophisticated electronic distributed control
system of instrumentation. The dried Carbon Black is
lifted by a bucket elevator and passed through a scalper
screen to separate lumps from the product- and
a magnetic separator to separate accidental contamination
of Carbon Black by magnetic particles before
discharging into product storage tanks by product screw
conveyors. Lumps separated from the product are returned
for reprocessing.
The black is then packed into 25-kg
multi-wall paper bags, polyethylene bags or super-sacks
for dispatch to customers. The packing of paper bags/
polyethylene bags are achieved by fluidising of Carbon
Black and super-sacks by gravity fill.
Carbon
Black manufacture: Process flow diagram
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